.灰星鲨肝油中角鲨烯的分离与鉴定[J].中国海洋药物,2004,23(3):34-35. |
灰星鲨肝油中角鲨烯的分离与鉴定 |
Separation and identification of squalene in liver oil from Mustelus griseus |
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中文关键词: 灰星鲨 肝油 角鲨烯 分离 鉴定 |
English Keywords:Mustelus griseus (Pietschmann),liver oil,squalene,separation,identification |
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中文摘要: |
应用硝酸银一硅胶薄层色谱的分离技术从灰星鲨肝油的烃类部分分离得到角鲨烯纯样品(99.9%),并用MS,1^H—NMR,13^C-NMR对其进行了鉴定。 |
English Summary: |
The pure squalene(99.9%) was separated from liver oil of Mustelus griseus(Pietschmann) by TLC on silver nitrate-impregnated silica gel. The structure of squalene was confirmed by MS, ~1H-NMR and ~(13)C-NMR techniques. |
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